4FSC
Crystal Structure of Bacillus thuringiensis PlcR in its apo form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2011-12-02 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.98011 |
Spacegroup name | P 31 |
Unit cell lengths | 99.589, 99.589, 137.850 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 53.840 - 3.650 |
R-factor | 0.24 |
Rwork | 0.238 |
R-free | 0.27630 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2qfc |
RMSD bond length | 0.008 |
RMSD bond angle | 1.060 |
Data reduction software | MOSFLM |
Data scaling software | SCALA (3.3.20) |
Phasing software | PHASER (2.3.0) |
Refinement software | BUSTER-TNT |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 86.247 | 53.843 | 3.850 |
High resolution limit [Å] | 3.650 | 11.540 | 3.650 |
Rmerge | 0.073 | 0.036 | 0.533 |
Number of reflections | 16981 | ||
<I/σ(I)> | 9.8 | 10.2 | 1.4 |
Completeness [%] | 99.7 | 99.2 | 98.9 |
Redundancy | 4.6 | 4.7 | 4.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 291.15 | 0.1M Sodium Chloride, 0.1M tri-Sodium citrate, 40% PEG400, pH 5.6, VAPOR DIFFUSION, HANGING DROP, temperature 291.15K |