4FQJ
Influenza B/Florida/4/2006 hemagglutinin Fab CR8071 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL11-1 |
Synchrotron site | SSRL |
Beamline | BL11-1 |
Detector technology | CCD |
Detector | MARMOSAIC 325 mm CCD |
Wavelength(s) | 0.9795 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 45.570, 111.930, 168.260 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.597 - 2.500 |
R-factor | 0.2323 |
Rwork | 0.230 |
R-free | 0.26540 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB ENTRIES 2RFT AND 3N9G |
RMSD bond length | 0.009 |
RMSD bond angle | 1.287 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.7.2_869)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.000 | 2.600 |
High resolution limit [Å] | 2.500 | 2.500 |
Number of reflections | 30377 | |
<I/σ(I)> | 15.6 | 2.4 |
Completeness [%] | 98.9 | 99.2 |
Redundancy | 5.6 | 6.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 295 | 20% PEG3350, 200 mM sodium sulfate, pH 8.0, VAPOR DIFFUSION, SITTING DROP, temperature 295K |