4FO7
Pseudomonas aeruginosa MetAP, in Mn form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-BM |
Synchrotron site | APS |
Beamline | 19-BM |
Detector technology | CCD |
Detector | ADSC QUANTUM 210 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 85.020, 111.422, 140.165 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 35.800 - 1.800 |
R-factor | 0.1941 |
Rwork | 0.192 |
R-free | 0.23040 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.031 |
RMSD bond angle | 2.574 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER (2.2.1) |
Refinement software | REFMAC |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.830 |
High resolution limit [Å] | 1.800 | 4.880 | 1.800 |
Rmerge | 0.090 | 0.057 | 0.424 |
Number of reflections | 114152 | ||
<I/σ(I)> | 12.3 | ||
Completeness [%] | 92.4 | 88.4 | 73.4 |
Redundancy | 4.2 | 5.2 | 1.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | hanging drop vapor diffusion | 7.5 | 100 mM HEPES, 70% MPD, pH 7.5, hanging drop vapor diffusion |