4FLB
CID of human RPRD2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-10-15 |
Detector | RIGAKU SATURN A200 |
Wavelength(s) | 1.5418 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 40.339, 40.339, 145.750 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.540 - 1.802 |
R-factor | 0.177 |
Rwork | 0.175 |
R-free | 0.21620 |
Structure solution method | SAD |
RMSD bond length | 0.015 |
RMSD bond angle | 1.441 |
Data reduction software | XDS |
Data scaling software | SCALA (CCP4_3.3.20) |
Phasing software | SHELX |
Refinement software | REFMAC (5.7.0027) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 28.540 | 28.520 | 1.900 |
High resolution limit [Å] | 1.800 | 5.700 | 1.800 |
Rmerge | 0.093 | 0.030 | 0.750 |
Total number of observations | 4239 | 20732 | |
Number of reflections | 11740 | ||
<I/σ(I)> | 25.0113 | ||
Completeness [%] | 98.9 | 98.63 | 97.08 |
Redundancy | 12.46 | 9.34 | 12.73 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 5.5 | 291 | 25% PEG-3350, 0.2M ammounium sulfate, 0.1M sodium cacodylate, praseodymium(III) acetate, pH 5.5, vapor diffusion, temperature 291K |