Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.3.1 |
Synchrotron site | ALS |
Beamline | 8.3.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-03-29 |
Detector | ADSC QUANTUM 210 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 51.205, 105.409, 110.473 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 55.240 - 2.650 |
R-factor | 0.262 |
Rwork | 0.259 |
R-free | 0.31500 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.004 |
RMSD bond angle | 0.816 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHENIX |
Refinement software | PHENIX ((phenix.refine: 1.7.3_928)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 76.263 | 2.720 |
High resolution limit [Å] | 2.650 | 2.650 |
Number of reflections | 17913 | |
Completeness [%] | 99.4 | 98.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6 | 277 | 100MM BISTRIS AT PH 6.0, 12.5% 2,5-HEXANEDIOL, AND 12% PEG3350, VAPOR DIFFUSION, SITTING DROP, temperature 277K |