4FJM

RB69 DNA polymerase ternary complex with dCTP/dA

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 24-ID-E
Synchrotron site	APS
Beamline	24-ID-E
Temperature [K]	110
Detector technology	CCD
Collection date	2011-10-15
Detector	APEX II CCD
Wavelength(s)	0.97
Spacegroup name	P 21 21 21
Unit cell lengths	75.238, 119.744, 130.297
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	45.550 - 2.020
R-factor	0.18989
Rwork	0.188
R-free	0.23192
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	1.190
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	AMoRE
Refinement software	REFMAC (5.5.0109)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.090
High resolution limit [Å]	2.020	2.020
Number of reflections	72632
Completeness [%]	96.0	98.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1