4FHN
Nup37-Nup120 full-length complex from Schizosaccharomyces pombe
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-02-19 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9792 |
Spacegroup name | P 63 2 2 |
Unit cell lengths | 329.999, 329.999, 350.262 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 95.117 - 6.989 |
R-factor | 0.2884 |
Rwork | 0.285 |
R-free | 0.34560 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.267 |
Data scaling software | SCALA (3.3.20) |
Refinement software | PHENIX (1.7.3_928) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 95.117 | 95.117 | 7.230 |
High resolution limit [Å] | 6.984 | 27.050 | 6.980 |
Rmerge | 0.026 | 0.026 | |
Total number of observations | 5905 | 31522 | |
Number of reflections | 18313 | ||
<I/σ(I)> | 15.2 | 11.4 | 0.3 |
Completeness [%] | 99.5 | 95.5 | 95.9 |
Redundancy | 22.4 | 16.2 | 18.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 291 | 100 mM Bis-Tris/HCl pH 5.75-6.5, 1.75-2.25 M NaCl , VAPOR DIFFUSION, HANGING DROP, temperature 291.0K |