4FHL
Nucleoporin Nup37 from Schizosaccharomyces pombe
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-06-19 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9792 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 131.726, 131.726, 117.970 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.553 - 2.600 |
R-factor | 0.1769 |
Rwork | 0.176 |
R-free | 0.18970 |
Structure solution method | SAD |
RMSD bond length | 0.003 |
RMSD bond angle | 0.834 |
Data scaling software | SCALA (3.3.20) |
Refinement software | PHENIX (1.8_1063) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 46.553 | 46.553 | 2.690 |
High resolution limit [Å] | 2.600 | 10.070 | 2.600 |
Rmerge | 0.011 | 0.011 | |
Total number of observations | 4863 | 30168 | |
Number of reflections | 32471 | ||
<I/σ(I)> | 16.9 | 15.4 | 0.7 |
Completeness [%] | 100.0 | 98.6 | 100 |
Redundancy | 9.5 | 7.5 | 9.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.75 | 303 | 100 mM Tris/HCl pH 7.75-8.25, 4% (v/v) 1,4-butanediol, 400-500 mM Li2SO4 , VAPOR DIFFUSION, HANGING DROP, temperature 303.0K |