4FH0
Crystal Structure of Human BinCARD CARD, double mutant F16M/L66M SeMet form
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-07-09 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9537, 0.9797, 0.9795 |
Spacegroup name | P 1 |
Unit cell lengths | 32.196, 36.669, 43.276 |
Unit cell angles | 108.54, 90.30, 111.01 |
Refinement procedure
Resolution | 27.724 - 1.400 |
R-factor | 0.1395 |
Rwork | 0.137 |
R-free | 0.17720 |
Structure solution method | MAD |
RMSD bond length | 0.010 |
RMSD bond angle | 1.303 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | SHARP |
Refinement software | PHENIX (1.7.2_869) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 32.139 | 1.470 |
High resolution limit [Å] | 1.250 | 1.400 |
Rmerge | 0.080 | 0.580 |
Number of reflections | 45785 | |
<I/σ(I)> | 16.2 | 4.4 |
Completeness [%] | 99.9 | 92.4 |
Redundancy | 7.1 | 7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6.5 | 298 | Bis-Tris pH 6.5, ammonium sulfate, PEG 3350, VAPOR DIFFUSION, temperature 298K |