4FCX
S.pombe Mre11 apoenzym
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-01-01 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 76.408, 82.262, 164.296 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 21.842 - 3.000 |
R-factor | 0.2324 |
Rwork | 0.227 |
R-free | 0.28580 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.210 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.7.3_928) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.000 | 3.180 |
High resolution limit [Å] | 3.000 | 3.000 |
Number of reflections | 21028 | |
Completeness [%] | 98.0 | 97.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 20mM HEPES 300mM NaCl, 0.1mM EDTA, 1mM MnCl2, 2mM beta-mercaptoethanol, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |