4F8V
Crystal structure of the bacterial ribosomal decoding site in complex with sisomicin (P21212 form)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL38B1 |
Synchrotron site | SPring-8 |
Beamline | BL38B1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-07-13 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 31.650, 107.650, 48.860 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.500 - 2.800 |
Rwork | 0.226 |
R-free | 0.26500 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.025 |
Data reduction software | CrystalClear |
Data scaling software | CrystalClear |
Phasing software | PHENIX |
Refinement software | CNS (1.3) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 44.500 |
High resolution limit [Å] | 2.800 |
Number of reflections | 4352 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 303 | Na Cacodylate, Spermine, NaCl, MPD , pH 7, VAPOR DIFFUSION, HANGING DROP, temperature 303K |