4F44
Neurotrophin p75NTR intracellular domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-10-09 |
Detector | RIGAKU SATURN 70 |
Wavelength(s) | 1.5 |
Spacegroup name | P 32 |
Unit cell lengths | 53.372, 53.372, 73.486 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.560 - 2.400 |
R-factor | 0.23024 |
Rwork | 0.228 |
R-free | 0.28001 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ngr |
RMSD bond length | 0.010 |
RMSD bond angle | 1.111 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.490 |
High resolution limit [Å] | 2.400 | 2.400 |
Number of reflections | 8699 | |
Completeness [%] | 84.0 | 84 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 277 | 0.1M Bis-Tris propane, 1.4M sodium malonate, pH 7.0, VAPOR DIFFUSION, SITTING DROP, temperature 277K |