4F0M
UNACTIVATED RUBISCO with MAGNESIUM AND A WATER MOLECULE BOUND
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2004-01-17 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | I 4 2 2 |
Unit cell lengths | 136.325, 136.325, 121.524 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 96.230 - 2.250 |
R-factor | 0.16288 |
Rwork | 0.159 |
R-free | 0.23416 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3rub |
RMSD bond length | 0.019 |
RMSD bond angle | 1.774 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-3000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 96.230 | 2.300 |
High resolution limit [Å] | 2.250 | 2.250 |
Rmerge | 0.101 | 0.751 |
Number of reflections | 27220 | |
<I/σ(I)> | 12.1 | 1.3 |
Completeness [%] | 98.9 | 93.1 |
Redundancy | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.5 | 298 | 0.05 M potassium phosphate, 26% Ammonium Sulfate, pH 7.5, VAPOR DIFFUSION, temperature 298.0K |