4F0H
UNACTIVATED RUBISCO with OXYGEN BOUND
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 298 |
Detector technology | IMAGE PLATE |
Collection date | 2003-11-27 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | I 4 2 2 |
Unit cell lengths | 136.440, 136.440, 121.670 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.000 - 1.960 |
R-factor | 0.16643 |
Rwork | 0.163 |
R-free | 0.22336 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3rub |
RMSD bond length | 0.021 |
RMSD bond angle | 1.906 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.010 |
High resolution limit [Å] | 1.960 | 1.960 |
Rmerge | 0.045 | 0.330 |
Number of reflections | 37497 | |
<I/σ(I)> | 25 | |
Completeness [%] | 94.2 | 71 |
Redundancy | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.5 | 298 | 0.05 M potassium phosphate, 26% Ammonium Sulfate, pH 7.5, VAPOR DIFFUSION, temperature 298.0K |