4ETI
Crystal Structure of YwlE from Bacillus subtilis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BSRF BEAMLINE 3W1A |
Synchrotron site | BSRF |
Beamline | 3W1A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-02-01 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 1.0000 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 84.736, 38.764, 40.463 |
Unit cell angles | 90.00, 91.12, 90.00 |
Refinement procedure
Resolution | 18.917 - 1.800 |
R-factor | 0.1808 |
Rwork | 0.178 |
R-free | 0.20130 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1zgg |
RMSD bond length | 0.003 |
RMSD bond angle | 0.769 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX ((phenix.refine: 1.7.3_928)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.000 | 1.900 |
High resolution limit [Å] | 1.800 | 1.800 |
Number of reflections | 11539 | |
Completeness [%] | 93.4 | 93.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 291 | 0.2M HCOONa, 20% PEG 3350, 0.1M spermidine, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 291K |