4EPU
Ang1 fibrinogen-related domain (FReD)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-D |
Synchrotron site | APS |
Beamline | 21-ID-D |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2011-07-31 |
Detector | MAR scanner 300 mm plate |
Wavelength(s) | 1.0781 |
Spacegroup name | P 64 |
Unit cell lengths | 80.903, 80.903, 186.087 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 46.443 - 2.098 |
R-factor | 0.1835 |
Rwork | 0.183 |
R-free | 0.20080 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1z3s |
RMSD bond length | 0.007 |
RMSD bond angle | 1.075 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.7_650) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.098 |
Number of reflections | 39116 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 291 | 0.1M PIPES pH 6.5, 0.2M NaCl, 2M ammonium sulfate, VAPOR DIFFUSION, SITTING DROP, temperature 291K |