4EGZ
Crystal Structure of AraR(DBD) in complex with operator ORR3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM14 |
Synchrotron site | ESRF |
Beamline | BM14 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-07-01 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 1.0 |
Spacegroup name | P 43 |
Unit cell lengths | 46.160, 46.160, 171.200 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.629 - 2.300 |
R-factor | 0.2224 |
Rwork | 0.220 |
R-free | 0.27120 |
Structure solution method | SAD |
RMSD bond length | 0.010 |
RMSD bond angle | 1.208 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SHELXS |
Refinement software | REFMAC (5.5.0072) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.300 |
Completeness [%] | 99.0 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.2 | 298 | 0.1M sodium acetate, 200mM KCl, 25% PEG 8000, pH 4.2, VAPOR DIFFUSION, HANGING DROP, temperature 298K |