4EF3
Multicopper Oxidase CueO (Citrate buffer)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL26B2 |
Synchrotron site | SPring-8 |
Beamline | BL26B2 |
Wavelength(s) | 0.8000 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 50.282, 91.239, 59.589 |
Unit cell angles | 90.00, 112.87, 90.00 |
Refinement procedure
Resolution | 17.600 - 1.900 |
R-factor | 0.15366 |
Rwork | 0.152 |
R-free | 0.18399 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.154 |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.900 |
Number of reflections | 38421 |
Completeness [%] | 98.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |