4EDL
Crystal structure of beta-parvin CH2 domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X25 |
Synchrotron site | NSLS |
Beamline | X25 |
Temperature [K] | 173 |
Detector technology | PIXEL |
Collection date | 2011-10-21 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 1.1 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 80.893, 52.584, 82.331 |
Unit cell angles | 90.00, 101.49, 90.00 |
Refinement procedure
Resolution | 50.000 - 2.100 |
R-factor | 0.2176 |
Rwork | 0.215 |
R-free | 0.26600 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.297 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.180 |
High resolution limit [Å] | 2.100 | 2.100 |
Number of reflections | 39650 | |
<I/σ(I)> | 14.011 | 2.155 |
Completeness [%] | 99.4 | 97.7 |
Redundancy | 2.9 | 2.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 18% PEG 4000, 0.1M sodium citrate, 3% isopropanol, VAPOR DIFFUSION, HANGING DROP, temperature 298K |