4EBB
Structure of DPP2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 93 |
Detector technology | CCD |
Collection date | 2005-07-15 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.97 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 61.089, 96.447, 192.137 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.770 - 2.000 |
R-factor | 0.20959 |
Rwork | 0.208 |
R-free | 0.22997 |
Structure solution method | SAD |
RMSD bond length | 0.006 |
RMSD bond angle | 0.864 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SHARP |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.770 | 2.052 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.079 | 0.475 |
Number of reflections | 72860 | |
<I/σ(I)> | 20 | 2 |
Completeness [%] | 98.9 | 96.77 |
Redundancy | 3.4 | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 295 | 0.1M sodium acetate, 0.05M zinc acetate, 5% PEG3350, pH 4.6, VAPOR DIFFUSION, HANGING DROP, temperature 295K |