4E6F
Crystal structure of a DUF4468 family protein (BACOVA_04320) from Bacteroides ovatus ATCC 8483 at 1.49 A resolution
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL11-1 |
Synchrotron site | SSRL |
Beamline | BL11-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-02-08 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97972,0.91837,0.97917 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 49.237, 89.078, 52.586 |
Unit cell angles | 90.00, 105.49, 90.00 |
Refinement procedure
Resolution | 47.449 - 1.490 |
R-factor | 0.1614 |
Rwork | 0.160 |
R-free | 0.18000 |
Structure solution method | MAD |
RMSD bond length | 0.010 |
RMSD bond angle | 0.970 |
Data reduction software | XDS |
Data scaling software | XSCALE (December 29, 2011) |
Phasing software | SHELX |
Refinement software | BUSTER-TNT (2.10.0) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 47.449 | 47.449 | 1.540 |
High resolution limit [Å] | 1.490 | 3.210 | 1.490 |
Rmerge | 0.054 | 0.028 | 0.546 |
Number of reflections | 69985 | 7051 | 6594 |
<I/σ(I)> | 12.94 | 35 | 2.19 |
Completeness [%] | 98.1 | 97 | 98 |
Redundancy | 3.42 | 3.36 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.20M potassium nitrate, 20.00% polyethylene glycol 3350, NANODROP, VAPOR DIFFUSION, SITTING DROP, temperature 293K |