Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

4E4Y

The crystal structure of a short chain dehydrogenase family protein from Francisella tularensis subsp. tularensis SCHU S4

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 19-ID
Synchrotron siteAPS
Beamline19-ID
Temperature [K]100
Detector technologyCCD
Collection date2010-06-07
DetectorADSC QUANTUM 315
Wavelength(s)0.97932
Spacegroup nameI 2 2 2
Unit cell lengths57.698, 79.260, 103.162
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution34.598 - 1.803
R-factor0.1642
Rwork0.162
R-free0.20360
Structure solution methodSAD
RMSD bond length0.006
RMSD bond angle1.024
Data reduction softwareHKL-3000
Data scaling softwareHKL-3000
Phasing softwareSHELXD
Refinement softwarePHENIX ((phenix.refine: 1.7.1_743))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]35.0001.830
High resolution limit [Å]1.8001.800
Rmerge0.0790.472
Number of reflections21819
<I/σ(I)>34.12.7
Completeness [%]98.6100
Redundancy9.49
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP6.52890.1M Bis-Tris, 2.0M Ammonium sulfate, pH 6.5, VAPOR DIFFUSION, SITTING DROP, temperature 289K

226707

PDB entries from 2024-10-30

PDB statisticsPDBj update infoContact PDBjnumon