Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | MACSCIENCE |
Temperature [K] | 293 |
Detector technology | AREA DETECTOR |
Collection date | 2001-01-02 |
Detector | SIEMENS HI-STAR |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 65.443, 76.990, 143.517 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.634 - 2.100 |
R-factor | 0.1653 |
Rwork | 0.163 |
R-free | 0.20570 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1qaz |
RMSD bond length | 0.012 |
RMSD bond angle | 1.326 |
Data reduction software | SAINT |
Data scaling software | SAINT |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.634 | 2.220 |
High resolution limit [Å] | 2.100 | 2.100 |
Number of reflections | 41806 | |
<I/σ(I)> | 12.1 | 2.6 |
Completeness [%] | 97.0 | 93.2 |
Redundancy | 4.45 | 2.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 293 | 24%(W/V) PEG4000, 0.3M AMMONIUM ACETATE, 0.1M SODIUM CITRATE, pH 5.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |