4DZL
A de novo designed Coiled Coil CC-Tri
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-05-17 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.7 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 102.761, 108.441, 41.608 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.420 - 2.300 |
R-factor | 0.24998 |
Rwork | 0.248 |
R-free | 0.28759 |
Structure solution method | SAD |
RMSD bond length | 0.008 |
RMSD bond angle | 1.021 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHENIX |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.400 |
High resolution limit [Å] | 2.300 | 2.300 |
Number of reflections | 21306 | |
Completeness [%] | 99.6 | 99.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 0.2 M C4H4KNaO6, 20 % w/v PEG 3350, VAPOR DIFFUSION, SITTING DROP, temperature 291K |