4DZB
Mucosal-associated invariant T cell receptor, Valpha7.2Jalpha33-Vbeta2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-11-10 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.95453 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 41.962, 64.515, 155.120 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 1.700 |
R-factor | 0.19264 |
Rwork | 0.191 |
R-free | 0.23063 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2nx5 |
RMSD bond length | 0.014 |
RMSD bond angle | 1.500 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.790 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.093 | 0.773 |
Number of reflections | 44624 | |
<I/σ(I)> | 13.7 | 2.5 |
Completeness [%] | 97.1 | 92.6 |
Redundancy | 7.6 | 7.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5 | 298 | 25% PEG 1500, 0.1M MIB buffer (sodium malonate, imidazole, boric acid), VAPOR DIFFUSION, HANGING DROP, temperature 298K |