4DYQ
High resolution crystal structure of terminase small subunit gp1 of the bacterial virus sf6
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL7-1 |
Synchrotron site | SSRL |
Beamline | BL7-1 |
Temperature [K] | 298 |
Detector technology | CCD |
Collection date | 2009-07-02 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97946 |
Spacegroup name | P 4 21 2 |
Unit cell lengths | 88.705, 88.705, 72.394 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.125 - 1.502 |
R-factor | 0.178 |
Rwork | 0.177 |
R-free | 0.20200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3hef |
RMSD bond length | 0.005 |
RMSD bond angle | 0.891 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHENIX |
Refinement software | PHENIX ((phenix.refine: 1.6.2_432)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.550 |
High resolution limit [Å] | 1.500 | 1.500 |
Rmerge | 0.044 | 0.503 |
Number of reflections | 45628 | |
<I/σ(I)> | 50.183 | 2.8 |
Completeness [%] | 97.9 | 97.6 |
Redundancy | 6.7 | 6.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.4 | 293 | 1.2M NAH2PO4/0.8M K2HPO4, 0.2M Li2SO4, pH 6.4, VAPOR DIFFUSION, HANGING DROP, temperature 293K |