4DYA

Crystal Structure of WSN/A Influenza Nucleoprotein with BMS-885986 Ligand Bound

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Detector technology	PIXEL
Detector	PSI PILATUS 6M
Spacegroup name	P 21 3
Unit cell lengths	145.496, 145.496, 145.496
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	48.510 - 2.750
R-factor	0.2537
Rwork	0.252
R-free	0.29760
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.006
RMSD bond angle	0.876
Data scaling software	XSCALE
Refinement software	REFMAC

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	102.881		2.930
High resolution limit [Å]	2.750	18.540	2.750
Rmerge	0.103	0.022	0.764
Number of reflections	26867	95	4499
<I/σ(I)>	15.61	57.59	2.43
Completeness [%]	99.7	88	99.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1