4DWL
Avd molecule from Bordetella bacteriophage DGR
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.2 |
Synchrotron site | ALS |
Beamline | 5.0.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-06-30 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97941, 0.97950, 0.97630 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 54.317, 63.072, 105.295 |
Unit cell angles | 90.00, 103.77, 90.00 |
Refinement procedure
Resolution | 42.910 - 2.690 |
R-factor | 0.197 |
Rwork | 0.194 |
R-free | 0.24390 |
Structure solution method | MAD |
RMSD bond length | 0.009 |
RMSD bond angle | 1.169 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SOLVE |
Refinement software | PHENIX ((phenix.refine: 1.6_289)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.820 | 2.540 |
High resolution limit [Å] | 2.500 | 2.750 | 2.500 |
Rmerge | 0.093 | ||
Number of reflections | 43542 | ||
Completeness [%] | 92.3 | 87.5 | 66.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 298 | 20% PEG 3350, 0.2M magnesium chloride, 0.4M barium chloride, 0.1M Bis-Tris, pH 6.0, VAPOR DIFFUSION, HANGING DROP, temperature 298.0K |