Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2005-04-28 |
| Detector | MARMOSAIC 225 mm CCD |
| Wavelength(s) | 0.90 |
| Spacegroup name | P 31 2 1 |
| Unit cell lengths | 84.670, 84.670, 58.300 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 45.630 - 1.300 |
| R-factor | 0.1376 |
| Rwork | 0.136 |
| R-free | 0.16800 |
| Structure solution method | SAD |
| RMSD bond length | 0.019 |
| RMSD bond angle | 1.897 |
| Data scaling software | XSCALE |
| Phasing software | SHELX |
| Refinement software | REFMAC |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 45.630 | 1.400 | |
| High resolution limit [Å] | 1.300 | 10.000 | 1.300 |
| Rmerge | 0.038 | 0.012 | 0.012 |
| Number of reflections | 59436 | 152 | 11723 |
| <I/σ(I)> | 30.22 | 141.12 | 2.12 |
| Completeness [%] | 99.9 | 93.8 | 99.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 4 | 293 | 0.1 mM Na+ acetate, 40% PEG 400, pH 4.0, vapor diffusion, hanging drop, temperature 293K |
