4DT1
Crystal structure of the Psy3-Csm2 complex
Experimental procedure
Experimental method | SINGLE WAVELENGHT |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-10-15 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 1.0 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 135.123, 50.433, 76.833 |
Unit cell angles | 90.00, 103.17, 90.00 |
Refinement procedure
Resolution | 33.094 - 1.899 |
R-factor | 0.1943 |
Rwork | 0.192 |
R-free | 0.22950 |
Structure solution method | MAD |
RMSD bond length | 0.007 |
RMSD bond angle | 0.990 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | PHENIX ((phenix.refine: 1.6_289)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.970 |
High resolution limit [Å] | 1.899 | 1.899 |
Number of reflections | 38738 | |
Completeness [%] | 96.6 | 84.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 285 | 100mM Tris-HCl, 10% Glycerol, 14% ethanol, pH 8.0, VAPOR DIFFUSION, HANGING DROP, temperature 285K |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 285 | 100mM Tris-HCl, 10% Glycerol, 14% ethanol, pH 8.0, VAPOR DIFFUSION, HANGING DROP, temperature 285K |