4DSY

Crystal structure of red kidney bean purple acid phosphatase in complex with Maybridge fragment CC24201

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	AUSTRALIAN SYNCHROTRON BEAMLINE MX2
Synchrotron site	Australian Synchrotron
Beamline	MX2
Detector technology	CCD
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.9
Spacegroup name	P 31 2 1
Unit cell lengths	127.705, 127.705, 299.761
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	19.864 - 2.300
R-factor	0.1636
Rwork	0.161
R-free	0.20750
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	1.061
Refinement software	PHENIX ((phenix.refine: 1.7_650))

Data quality characteristics

	Overall
Low resolution limit [Å]	99.663
High resolution limit [Å]	2.300
Number of reflections	125955

Crystallization Conditions

crystal ID	method	pH	temperature	details
1