4DOQ
Crystal structure of the complex of Porcine Pancreatic Trypsin with 1/2SLPI
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E+ SUPERBRIGHT |
Temperature [K] | 298 |
Detector technology | IMAGE PLATE |
Collection date | 2005-10-10 |
Detector | RIGAKU |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 40.535, 118.610, 93.393 |
Unit cell angles | 90.00, 90.74, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 93.250 | 2.050 |
High resolution limit [Å] | 2.000 | 2.000 |
Number of reflections | 57599 | |
Completeness [%] | 96.8 | 95.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 298 | 25% PEG4000, 0.1M Na-Citrate, 200mM Ammonium Sulfate, pH 7.5, VAPOR DIFFUSION, SITTING DROP, temperature 298K |