4DIX
Crystal structure of the Ig-PH domain of actin-binding protein SCAB1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2008-06-20 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 76.329, 76.329, 161.856 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.780 - 1.700 |
R-factor | 0.2081 |
Rwork | 0.207 |
R-free | 0.23300 |
Structure solution method | SAD |
RMSD bond length | 0.007 |
RMSD bond angle | 1.200 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SHARP |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 20.000 | 20.000 | 1.730 |
High resolution limit [Å] | 1.700 | 4.600 | 1.700 |
Rmerge | 0.050 | 0.032 | 0.565 |
Number of reflections | 58454 | ||
<I/σ(I)> | 19.6 | ||
Completeness [%] | 95.9 | 98.9 | 92.8 |
Redundancy | 10.8 | 9.5 | 10.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.4 | 293 | 2.0M sodium malonate, pH 6.4, vapor diffusion, hanging drop, temperature 293K |