4DH4
Macrophage migration inhibitory factor Toxoplasma gondii
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 200 |
Detector technology | CCD |
Collection date | 2009-02-14 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97630 |
Spacegroup name | H 3 2 |
Unit cell lengths | 58.730, 58.730, 183.971 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 49.000 - 1.820 |
R-factor | 0.19486 |
Rwork | 0.193 |
R-free | 0.23107 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.066 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.000 | 1.920 |
High resolution limit [Å] | 1.820 | 1.820 |
Rmerge | 0.083 | 0.395 |
Number of reflections | 11318 | |
<I/σ(I)> | 5.8 | |
Completeness [%] | 100.0 | 100 |
Redundancy | 10.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 277 | 1.82M ammonium sulphate, 100mM Tris pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 277K |