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4DD2

EVAL processed HEWL, carboplatin aqueous glycerol

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU MICROMAX-007
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2010-03-02
DetectorRIGAKU RAXIS IV
Wavelength(s)1.5418
Spacegroup nameP 43 21 2
Unit cell lengths78.906, 78.906, 36.998
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution19.730 - 1.550
R-factor0.20244
Rwork0.200
R-free0.24505
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2w1y
RMSD bond length0.019
RMSD bond angle2.072
Data reduction softwareEVAL15 (15)
Data scaling softwareEVAL15 (15)
Phasing softwarePHASER (MR)
Refinement softwareREFMAC (5.6.0117)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]19.7301.600
High resolution limit [Å]1.5501.550
Rmerge0.0630.456
Number of reflections13707
<I/σ(I)>30.12.1
Completeness [%]94.794.9
Redundancy18.84.2
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1BATCH4.7295HEWL co-crystallized with carboplatin in 1 mL 0.05 M sodium acetate buffer and 1 mL 10% sodium chloride aqueous media, pH 4.7, BATCH, temperature 295K

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