4DBG
Crystal structure of HOIL-1L-UBL complexed with a HOIP-UBA derivative
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL44XU |
Synchrotron site | SPring-8 |
Beamline | BL44XU |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-02-16 |
Detector | Bruker DIP-6040 |
Wavelength(s) | 0.9000 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 64.973, 64.973, 161.291 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 56.270 - 2.710 |
R-factor | 0.2199 |
Rwork | 0.218 |
R-free | 0.25250 |
Structure solution method | MAD |
RMSD bond length | 0.018 |
RMSD bond angle | 1.785 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | SHARP |
Refinement software | REFMAC |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 300.000 | 300.000 | 2.800 |
High resolution limit [Å] | 2.700 | 5.820 | 2.700 |
Rmerge | 0.103 | 0.071 | 0.332 |
Number of reflections | 20666 | ||
<I/σ(I)> | 18.8 | ||
Completeness [%] | 99.9 | 99.5 | 100 |
Redundancy | 5.7 | 5.4 | 5.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 15%(w/v) PEG6000, 0.1M KCl, 0.1M HEPES-Na buffer, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 293.0K |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 15%(w/v) PEG6000, 0.1M KCl, 0.1M HEPES-Na buffer, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 293.0K |