4DB9
Designed Armadillo repeat protein (YIIIM3AIII)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | BRUKER AXS MICROSTAR |
Temperature [K] | 298 |
Detector technology | IMAGE PLATE |
Collection date | 2010-08-09 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.54 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 131.920, 228.880, 116.530 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 34.730 - 2.400 |
R-factor | 0.21282 |
Rwork | 0.211 |
R-free | 0.24579 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.036 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 34.730 |
High resolution limit [Å] | 2.400 |
Rmerge | 0.107 |
Number of reflections | 65534 |
<I/σ(I)> | 5.2 |
Completeness [%] | 100.0 |
Redundancy | 5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.03 | 293 | 1.55 M sodium malonate, pH 8.03, VAPOR DIFFUSION, SITTING DROP, temperature 293K |