4D81
Metallosphera sedula Vps4 crystal structure
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM14 |
Synchrotron site | ESRF |
Beamline | BM14 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-11-11 |
Detector | MARRESEARCH |
Spacegroup name | P 65 |
Unit cell lengths | 65.269, 65.269, 112.521 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 56.520 - 2.400 |
R-factor | 0.20971 |
Rwork | 0.207 |
R-free | 0.26283 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.012 |
RMSD bond angle | 1.572 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 56.500 | 2.490 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.060 | 0.630 |
Number of reflections | 12935 | |
<I/σ(I)> | 16.7 | 2.3 |
Completeness [%] | 99.7 | 99.7 |
Redundancy | 4.1 | 4.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8.8 | 40% (W/V) POLYETHYLENE GLYCOL 200 (PEG200) 100 MM TRIS-HCL BUFFER (PH 8.8) |