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4D7Y

Crystal structure of mouse C1QL1 globular domain

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I04
Synchrotron siteDiamond
BeamlineI04
Temperature [K]100
Detector technologyPIXEL
Collection date2014-06-21
DetectorDECTRIS PILATUS 6M
Spacegroup nameH 3
Unit cell lengths68.080, 68.080, 65.910
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution34.040 - 1.440
R-factor0.1415
Rwork0.140
R-free0.16930
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1c28
RMSD bond length0.006
RMSD bond angle1.096
Data reduction softwarexia2
Data scaling softwarexia2
Phasing softwarePHASER
Refinement softwarePHENIX ((PHENIX.REFINE))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]43.9401.480
High resolution limit [Å]1.4401.440
Rmerge0.0700.880
Number of reflections20630
<I/σ(I)>16.92
Completeness [%]100.099.9
Redundancy7.67.3
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
14.50.02M NICKEL(II) CHLORIDE HEXAHYDRATE, 0.02M MAGNESIUM CHLORIDE HEXAHYDRATE, 0.02M CADMIUM CHLORIDE HYDRATE, 0.1M SODIUM ACETATE TRIHYDRATE PH 4.5, 24% W/V POLYETHYLENE GLYCOL, MONOMETHYL ETHER 2,000

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