Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06DA |
| Synchrotron site | SLS |
| Beamline | X06DA |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2009-06-15 |
| Detector | MARRESEARCH |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 40.454, 87.420, 62.226 |
| Unit cell angles | 90.00, 91.46, 90.00 |
Refinement procedure
| Resolution | 40.441 - 1.482 |
| R-factor | 0.1926 |
| Rwork | 0.190 |
| R-free | 0.23900 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4a6p |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.213 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | AMoRE |
| Refinement software | PHENIX ((PHENIX.REFINE: 1.8.4_1496)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 43.710 | 1.570 |
| High resolution limit [Å] | 1.480 | 1.480 |
| Rmerge | 0.060 | 0.470 |
| Number of reflections | 126096 | |
| <I/σ(I)> | 8.76 | 2.02 |
| Completeness [%] | 88.1 | 89.4 |
| Redundancy | 1.92 | 1.92 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 5.8 | 60 MM NA2HPO4 PH 6.0, 15% PEG 1000 |
