4D6O
THE CRYSTAL STRUCTURE OF I-DMOI IN COMPLEX WITH ITS TARGET DNA AT 1H INCUBATION IN 5MM MG (STATE 2)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 2M-F |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 106.888, 70.672, 107.143 |
Unit cell angles | 90.00, 119.80, 90.00 |
Refinement procedure
Resolution | 46.489 - 2.200 |
R-factor | 0.1866 |
Rwork | 0.186 |
R-free | 0.22010 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB DENTRY 2VS7 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.159 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.490 | 2.320 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.060 | 0.420 |
Number of reflections | 70363 | |
<I/σ(I)> | 13.1 | 3.4 |
Completeness [%] | 99.6 | 100 |
Redundancy | 4.1 | 4.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.5 | pH 5.5 |