4D5E

Crystal Structure of recombinant wildtype CDH

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06DA
Synchrotron site	SLS
Beamline	X06DA
Temperature [K]	287
Detector technology	PIXEL
Collection date	2012-02-14
Detector	DECTRIS PILATUS 2M-F
Spacegroup name	P 41 21 2
Unit cell lengths	123.188, 123.188, 143.070
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	46.680 - 1.430
R-factor	0.12326
Rwork	0.122
R-free	0.14733
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.024
RMSD bond angle	2.315
Data reduction software	XDS
Data scaling software	SCALA
Refinement software	REFMAC (5.8.0069)

Data quality characteristics

	Overall
Low resolution limit [Å]	47.690
High resolution limit [Å]	1.430
Rmerge	0.100
Number of reflections	201517
<I/σ(I)>	16.1
Completeness [%]	100.0
Redundancy	10

Crystallization Conditions

crystal ID	method	pH	temperature	details
1