4D4O
Crystal Structure of the Kti11 Kti13 heterodimer Spacegroup P64
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, EMBL c/o DESY BEAMLINE P14 (MX2) |
Synchrotron site | PETRA III, EMBL c/o DESY |
Beamline | P14 (MX2) |
Temperature [K] | 100 |
Collection date | 2013-11-07 |
Spacegroup name | P 64 |
Unit cell lengths | 151.270, 151.270, 107.140 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 75.635 - 2.897 |
R-factor | 0.1991 |
Rwork | 0.198 |
R-free | 0.21880 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.004 |
RMSD bond angle | 0.627 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.970 |
High resolution limit [Å] | 2.900 | 2.900 |
Rmerge | 0.100 | |
Number of reflections | 30909 | |
<I/σ(I)> | 20.33 | 1.5 |
Completeness [%] | 99.4 | 94.1 |
Redundancy | 11.06 | 10 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 100 MM TRIS PH 7.4, 2 M LI2SO4 |