4D0M
Phosphatidylinositol 4-kinase III beta in a complex with Rab11a-GTP- gamma-S and the Rab-binding domain of FIP3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-02-09 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 199.504, 134.465, 294.328 |
Unit cell angles | 90.00, 90.33, 90.00 |
Refinement procedure
Resolution | 294.320 - 6.000 |
R-factor | 0.25888 |
Rwork | 0.253 |
R-free | 0.35946 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4d0l |
RMSD bond length | 0.012 |
RMSD bond angle | 1.366 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0069) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.880 | 6.270 |
High resolution limit [Å] | 6.000 | 6.000 |
Rmerge | 0.170 | 1.030 |
Number of reflections | 37822 | |
<I/σ(I)> | 17.8 | 2.2 |
Completeness [%] | 95.9 | 97 |
Redundancy | 5.6 | 5.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 16% PEG 6K, 0.01 M NA CITRATE |