4D07
DYNLL2 dynein light chain binds to an extended, unstructured linear motif of myosin 5a tail
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-11-09 |
Detector | ADSC QUANTUM 315r |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 45.160, 45.160, 204.010 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 204.010 - 1.850 |
R-factor | 0.19492 |
Rwork | 0.193 |
R-free | 0.23300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1cmi |
RMSD bond length | 0.007 |
RMSD bond angle | 1.113 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0069) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.760 | 1.900 |
High resolution limit [Å] | 1.850 | 1.850 |
Rmerge | 0.100 | 0.700 |
Number of reflections | 11478 | |
<I/σ(I)> | 30.18 | 6.09 |
Completeness [%] | 99.8 | 100 |
Redundancy | 22 | 20 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 2.5UL PROTEIN PLUS 1UL RESERVOIR SOLUTION OF 1.8 M (NH4)2SO4, 0.02 M COCL2, 0.1 M MES PH 6.5 |