4CZ9
Structure of the sodium proton antiporter PaNhaP from Pyrococcus abyssii at pH 4.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-05-03 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 64 |
Unit cell lengths | 109.566, 109.566, 209.626 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 50.000 - 3.500 |
Rwork | 0.242 |
R-free | 0.26300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4cz8 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.720 |
High resolution limit [Å] | 3.500 | 3.500 |
Rmerge | 0.020 | 0.490 |
Number of reflections | 33232 | |
<I/σ(I)> | 19.9 | 1.9 |
Completeness [%] | 100.0 | 100 |
Redundancy | 9.2 | 9.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4 | pH 4.0 |