4CYW
Structure of the A_mallard_Sweden_51_2002 H10 Avian Haemmaglutinin in complex with human receptor analog 6-SLN
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04 |
| Synchrotron site | Diamond |
| Beamline | I04 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Detector | DECTRIS PILATUS |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 68.973, 215.446, 79.363 |
| Unit cell angles | 90.00, 104.91, 90.00 |
Refinement procedure
| Resolution | 107.720 - 2.600 |
| R-factor | 0.21067 |
| Rwork | 0.208 |
| R-free | 0.25402 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4cyv |
| RMSD bond length | 0.005 |
| RMSD bond angle | 1.008 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.850 | 2.660 |
| High resolution limit [Å] | 2.600 | 2.600 |
| Rmerge | 0.070 | 0.690 |
| Number of reflections | 67905 | |
| <I/σ(I)> | 11.8 | 1.8 |
| Completeness [%] | 99.1 | 99.8 |
| Redundancy | 3.6 | 3.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 18% PEG 2000MME AND 0.1 M BICINE PH 9.0 |
