4CYJ
Chaetomium thermophilum Pan2:Pan3 complex
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-4 |
| Synchrotron site | ESRF |
| Beamline | ID14-4 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Detector | DECTRIS PIXEL |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 89.094, 145.359, 101.811 |
| Unit cell angles | 90.00, 94.86, 90.00 |
Refinement procedure
| Resolution | 47.890 - 2.590 |
| R-factor | 0.1849 |
| Rwork | 0.183 |
| R-free | 0.22060 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.146 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 100.000 | 2.680 |
| High resolution limit [Å] | 2.590 | 2.590 |
| Rmerge | 0.060 | 0.660 |
| Number of reflections | 80131 | |
| <I/σ(I)> | 12 | 1.77 |
| Completeness [%] | 99.8 | 99.7 |
| Redundancy | 6.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | SEE PUBLICATION FOR DETAILS |
