4CYI

Chaetomium thermophilum Pan3

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND
Synchrotron site	Diamond
Beamline	I03
Temperature [K]	100
Spacegroup name	P 1
Unit cell lengths	51.520, 146.040, 149.930
Unit cell angles	89.81, 81.13, 82.77

Refinement procedure

Resolution	52.212 - 2.420
R-factor	0.1925
Rwork	0.190
R-free	0.23430
Structure solution method	SAD
Starting model (for MR)	NONE
RMSD bond length	0.004
RMSD bond angle	0.875
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	SHARP
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	52.210	2.480
High resolution limit [Å]	2.420	2.420
Rmerge	0.040	0.360
Number of reflections	160956
<I/σ(I)>	14.3	2.4
Completeness [%]	98.5	98
Redundancy	7.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1				SEE MANUASCRIPT