4CYA
DpsA15 from Streptomyces coelicolor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 42 3 2 |
Unit cell lengths | 105.330, 105.330, 105.330 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 60.810 - 1.860 |
R-factor | 0.16036 |
Rwork | 0.159 |
R-free | 0.18007 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.021 |
RMSD bond angle | 1.777 |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 60.800 |
High resolution limit [Å] | 1.860 |
Rmerge | 0.080 |
Number of reflections | 17268 |
<I/σ(I)> | 19.8 |
Completeness [%] | 99.9 |
Redundancy | 14 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |